1010T入門套件
1010T入門套件旨在幫助初學者更快速理解電化學基礎知識並開始進行測量,並包含教材適合大學或學術機構使用。
循環伏安法
- 測定鐵氰化鉀的氧化還原電位與擴散係數。
電極作用面積的測定
- 計算工作電極的電化學活性面積、理解濃度–距離剖面、熟悉Cottrell equations與 Anson equations。
脈衝技術比較
- 比較不同的脈衝技術、測定未知水樣本中銅的含量。
不同 pH 下的低碳鋼腐蝕
- 測定低碳鋼在不同 pH 環境下的腐蝕速率。
電化學阻抗譜
- 對電阻與電容組成的網路進行 EIS 測試、使用等效電路模型擬合 EIS 數據,提取電阻與電容值。
Student and Teacher Manuals 學生與教師手冊
學生與教師手冊規劃完善,包含每個實驗的目標、所需設備、試劑與化學品(含配製說明)
逐步操作程序
我們還提供詳細的逐步操作程序,幫助使用者熟悉儀器與軟體的操作。這讓學習重點聚焦在理解實驗內容,而不是同時要摸索軟體操作。
數據分析問題
每本手冊均包含數據分析相關問題,而教師手冊則包含實驗的預期結果(如附圖所示)。教師可清楚了解學生應該觀察到的數據與他們在數據處理中應該計算出的結果。
Interface 1010T
Interface 1010T 是一款非常適合本科及研究所教學實驗室使用的恆電位儀。作為入門級恆電位儀,Interface 1010T 專為本科及研究所教學實驗室設計,提供所有必要功能,讓學生能夠進入物理與分析電化學的世界。它甚至還能支援高達 20 kHz 的電位控制式 EIS 測試。
物理電化學 – 技術如循環伏安法 (Cyclic Voltammetry)、計時安培法 (Chronoamperometry) 和計時電位法 (Chronopotentiometry)。
脈衝伏安法 – 技術如差分脈衝伏安法 (Differential Pulse Voltammetry)、正常脈衝伏安法 (Normal Pulse Voltammetry)、Osteryoung 方波伏安法 (Osteryoung Square Wave Voltammetry),以及相關的剝離分析技術。
電化學阻抗分析 (EIS) – 電位控制式 EIS,頻率最高可達 20 kHz。
Interface 1010T 可透過現場升級 (infield upgrade) 升級為功能完整的 Interface 1010E,讓您能先以低成本取得教學用恆電位儀,日後再升級為研究等級的恆電位儀,支援更廣泛的應用實驗。
入門套件內包含:
- Interface 1010T 恆電位儀/恆電流儀/零電阻電流計(ZRA)
- 五個實驗
- 數位版學生與教師手冊
- 電池與電極
這些實驗能幫助學生學習各種技術,從循環伏安法到脈衝技術、腐蝕測試,甚至是電化學阻抗譜(EIS)。
系統 |
|
恒電位儀 |
Yes |
恒電流儀 |
Yes |
零電阻電流表 |
Yes |
浮動(與大地隔離) |
Yes |
電極連接 |
2, 3, or 4 |
最大電流 |
± 100 mA |
電流範圍 |
6 (1 uA - 100 mA) |
電流範圍(包括內部增益) |
8 (10 nA - 100 mA) |
小電流解析度 |
0.3 pA |
最大應用電位 |
± 5 V |
上升時間 |
<1 μs |
最小時基 |
1 ms |
雜訊與漣波 |
<20 μV rms |
重量 |
2.4 kg |
尺寸 |
24 (W) x 6 (H) x 27 (D) cm |
|
|
控制放大器 |
|
相容電壓 |
±20 V (@ 1A) |
輸出電流 |
>±1 A |
速度設定 |
5 |
單一增益頻寬 |
980, 260, 40, 4, 0.4 kHz |
|
|
EIS測量 |
|
EIS 頻率 |
10 μHz - 20 kHz |
99% |
|
AC 振幅 |
2.33 V maximum
|
靜電計 |
|
輸入阻抗 |
>1012 Ω |
輸入電流(典型值) |
<20 pA |
頻寬 |
>10 MHz |
CMRR (共模拒次比) |
>80 dB (10 kHz) |
|
|
電位 |
|
應用精確度 |
±1 mV ±0.2% of setting |
應用解析度 |
200 μV, 50 μV, 12.5 μV/bit |
測量精確度 |
±1 mV ±0.3% of reading |
測量解析度 |
1 μV, 10 μV, 100 μV, 400 μV/bit |
|
|
電流 |
|
應用精確度 |
±5 pA ±0.3% of range |
應用解析度 |
0.0033% full-scale/bit |
|
|
測量電流 |
|
量測精確度 |
±5 pA ±0.3% of range |
量測解析度 |
0.0033% full-scale/bit |
頻寬 |
>10 MHz (1A - 100 μA) |
1010T Starter Package
The Interface 1010T Potentiostat/Galvanostat/ZRA and Starter Pack is designed to help people understand and start making measurements sooner.
Cyclic Voltammetry
- Determine the redox potential and diffusion coefficient of potassium ferricyanide.
Determination of Working Area of an Electrode
- Calculate the electroactive area of the WE. Understand concentration distance profiles. Familiarization with the Cottrell and Anson equations
Comparison of Pulse Techniques
- Compare different pulse techniques. Determine amount of copper in an unknown water sample
Corrosion of Mild Steel at different pHs.
- Determine the corrosion rates for mild steel at different pHs.
Electrochemical Impedance Spectroscopy
- Perform EIS on a network of resistors and capacitors. Model EIS data using an equivalent circuit to extra resistor and capacitor values.
Student and Teacher Manuals
Our student and teacher manuals are ideally laid out with goals of each experiment, necessary equipment, reagents and chemicals (including instructions for preparation).
Step-by-step Procedures
We also include detailed step-by-step procedures to help you become familiar with operation of the instrument and software. This helps keep the focus on learning the material versus having to simultaneously learn the software.
Data Analysis Questions
Each manual also includes questions regarding data analysis while the teacher’s manual includes the expected results of the experiments as shown on the right. You can see what each student should be seeing and also what they should be calculating in their data workup.
Interface 1010T
The Interface 1010T is a perfect potentiostat for use in undergraduate and graduate teaching labs. An entry-level potentiostat, the Interface 1010T is designed for undergraduate and graduate teaching labs providing all of the capabilities needed for getting students introduced to physical and analytical electrochemistry. It even provides for potentiostatic EIS up 20 kHz.
Physical Electrochemistry – Techniques such as cyclic voltammetry, chronoamperometry, and chronopotentiometry.
Pulse Voltammetry – Techniques such as differential pulse voltammetry, normal pulse voltammetry, Osteryoung square wave voltammetry, and associated stripping techniques.
Electrochemical Impedance Spectroscopy – Potentiostatic EIS up to 20 kHz.
The Interface 1010T can be upgraded to a fully-featured Interface 1010E with an infield upgrade, allowing you to get a low-cost potentiostat for teaching purposes that can later be upgraded to a fully-capable research-grade potentiostat able to perform experiments for a wide variety of applications.
The kit includes:
- Interface 1010T Potentiostat/Galvanostat/ZRA
- Five experiments
- Student and Teacher’s manuals (digital)
- Cells and electrodes
Experiments have been chosen to help learn a variety of techniques from cyclic voltammetry to pulse techniques to corrosion techniques and even electrochemical impedance spectroscopy (EIS).
SYSTEM |
|
Potentiostat | Yes |
Galvanostat | Yes |
Zero Resistance Ammeter | Yes |
Floating (Isolated from Earth Ground) | Yes |
Cell Connections | 2, 3, or 4 |
Maximum Current | ± 100 mA |
Current Ranges | 6 (1 uA - 100 mA) |
Current Ranges (including internal gain) |
8 (10 nA - 100 mA) |
Minimum Current Resolution | 0.3 pA |
Maximum Applied Potential | ± 5 V |
Rise Time | <1 μs |
Minimum Time Base | 1 ms |
Noise and Ripple | <20 μV rms |
Weight | 2.4 kg |
Dimensions | 24 (W) x 6 (H) x 27 (D) 27 cm |
CONTROL AMPLIFIER |
|
Compliance Voltage | ±20 V (@ 1A) |
Output Current | >±1 A |
Speed Settings | 5 |
Unity Gain Bandwidth | 980, 260, 40, 4, 0.4 kHz |
EIS MEASUREMENT |
|
EIS | 10 uHz - 20 kHz |
EIS Accuracy | 99% |
AC Amplitude | 2.33 V maximum 17.8 μV minimum |
ELECTROMETER |
|
Input Impedance | >1012 Ω |
Input Current (typical) | <20 pA |
Bandwidth | >10 MHz |
CMRR | >80 dB (10 kHz) >60 dB (1 MHz) |
POTENTIAL |
|
Applied Accuracy | ±1 mV ±0.2% of setting |
Applied Resolution | 200 μV, 50 μV, 12.5 μV/bit |
Measured Accuracy | ±1 mV ±0.3% of reading |
Measured Resolution | 1 μV, 10 μV, 100 μV, 400 μV/bit |
CURRENT |
|
Applied Accuracy | ±5 pA ±0.3% of range |
Applied Resolution | 0.0033% full-scale/bit |
MEASURED CURRENT |
|
Measured Accuracy | ±5 pA ±0.3% of range |
Measured Resolution | 0.0033% full-scale/bit |
Bandwidth |
>10 MHz (1A - 100 μA) |